Answer: The theoretical yield of aspirin is 4.14 g
Explanation:
To calculate the moles :
mass of acetic anhydride = 
According to stoichiometry :
1 mole of salycylic acid require 1 mole of acetic anhydride
Thus 0.023 moles of salycylic acid require=
of acetic anhydride
Thus salycylic acid is the limiting reagent as it limits the formation of product and acetic anhydride is the excess reagent.
As 1 mole of salycylic give = 1 mole of aspirin
Thus 0.023 moles of salycylic acid give = of aspirin
Mass of aspirin = 
Thus theoretical yield of aspirin is 4.14 g
Answer:
2%
Explanation:
oriented C-2, and (3) the minimizing of the number of ... (2) L. A. Mitscher, J. K. Paul, and L. Goldman,Experientia, 19, 195. (1963). ... SOzCeHiBr)3 in 147 ml. of anhydrous methanol containing 0.37 ... bicarbonate and saturated sodium chloride solution, and dried ... determined in 2% chloroform solution; infrared spectra on.
Answer:
The answer is below
Explanation:
The separation technique is used for separating immiscible liquids.
When separating, the stopper has to be removed when draining the lower layer so as to prevent a vacuum. If vacuum is allowed, the draining rate will reduce and stop.
The liquid should be mixed by shaking the funnel and then opening the stopcock so as the vent out gases.
When near interface between the layers, you should set your eye level so that you do not drain up to the second layer.
After completely draining the first layer, the second layer should be collected in a new flask.
After mixing the solutions in a separatory funnel, the stopper should be removed and the liquid should be mixed thoroughly and the layers allowed to separate. When you get close to the interface between the layers, get eye level with the funnel and slow the draining until the first layer is collected. Switch to a new flask to collect the second layer.
Explanation:
Significant figure is the measure of how accurately something can be measured. It carries meaning contributing to its measurement resolution. It is important to use proper number of significant figures to get a precise measurement. For example, if we use a meter stick then measurements like 0.874 meters, or 0.900 meters, are good because they indicate that we can measure to the nearest millimeter. Whereas a measurement like 0.8 does not tell that a meter stick can measure to the nearest millimeter.
