Aniline can be produced from nitro-benzene by reduction. When nitro-benzene reacts with tin (Sn) + hydrochloride acid (HCl) then aniline is produced. The Sn + HCl forms free hydrogen ions which converts the nitro group of the benzene ring to amine group, which is aniline. In place of Sn + HCl. One can use palladium (Pd) hydrogen mixture in presence of ethanol (EtOH). There produces a side product in this reaction which is cyclohexyl amine. The reaction can be shown as.
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Answer:
An unknown being weighed is hygroscopic. - operative error
One component of a mixture being analyzed quantitatively by gas chromatography reacts with the column packing. - methodic error
The tip of the pipet used in the analysis is broken. - instrumental error
In measuring the same peak heights of a chromatogram, two technicians each report different heights - operative error
Explanation:
In chemical analysis, operative errors are that largely introduced into the measurement because of variation of personal judgements of analysts. It is also a personal error that emanates solely due to the analyst.
A methodic error arises as a result of adopting defective experimental methods. For example, a column packing that reacts with a component of the mixture is used in the gas chromatography.
Instrument error refers to the error of a measuring instrument, for instance, the use of a pipette with a broken tip.
Answer:
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Explanation:
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