According to the question, the determined melting point of the compound is 112.5-113.0oC. When the solidified compound was retried, the melting point was found to be 133.6-154.5oC. This greater range higher than 112°C is caused by reusing samples leads to errors.
A pure sample is known by its sharp melting point. A pure sample does not melt over a large range. We can see this in the predetermined melting points of the pure sample(112.5-113.0oC).
However, reusing a sample introduces errors because the pure sample may become contaminated leading to a larger and higher range of melting point (133.6-154.5oC) which is far above 112°C.
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Answer:
0.823 M was the molarity of the KOH solution.
Explanation:
(Neutralization reaction)
To calculate the concentration of base , we use the equation given by neutralization reaction:

where,
are the n-factor, molarity and volume of acid which is 
are the n-factor, molarity and volume of base which is KOH.
We are given:

Putting values in above equation, we get:


0.823 M was the molarity of the KOH solution.
Some signs of a chemical change are a change in color and the formation of bubbles. The five conditions of chemical change: color chage, formation of a precipitate, formation of a gas, odor change, temperature change.