Cryo-EM is used to preserve and characterize cycled positive electrodes. Under regular cycling conditions, there isn't an intimate coating layer like CEI.A small electrical short can cause a stable conformal CEI to form in place. The conformal CEI's chemistry is revealed by EELS and cryo-(S)TEM.
It has been assumed that the intimate coating layer generated on the positive electrode, known as cathode electrolyte interphase (CEI), is crucial. However, there are still numerous questions about CEI. This results from the absence of useful instruments to evaluate the chemical and structural characteristics of these delicate interphases at the nanoscale. Here, using cryogenic electron microscopy, we establish a methodology to maintain the natural condition and directly see the interface on the positive electrode.
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Mass of methanol (CH3OH) = 1.922 g
Change in Temperature (t) = 4.20°C
Heat capacity of the bomb plus water = 10.4 KJ/oC
The heat absorbed by the bomb and water is equal to the product of the heat capacity and the temperature change.
Let’s assume that no heat is lost to the surroundings. First, let’s calculate the heat changes in the calorimeter. This is calculated using the formula shown below:
qcal = Ccalt
Where, qcal = heat of reaction
Ccal = heat capacity of calorimeter
t = change in temperature of the sample
Now, let’s calculate qcal:
qcal = (10.4 kJ/°C)(4.20°C)
= 43.68 kJ
Always qsys = qcal + qrxn = 0,
qrxn = -43.68 kJ
The heat change of the reaction is - 43.68 kJ which is the heat released by the combustion of 1.922 g of CH3OH. Therefore, the conversion factor is:
Answer:
The molecular formula of X is C8H9NO2
Explanation:
Step 1: Data given
exact mass of 151.0640
Molar mass of C = 12 g/mol
Molar mass of H = 1.00783 g/mol
Molar mass of O = 15.9949 g/mol
Molar mass of N = 14.0031 g/mol
Step 2: Calculate molar mass of C7H5NO3
7*12 + 5*1.00783 + 14.0031 + 3*15.9949 = 151.02695 g/mol
Step 3: Calculate molar mass of C8H9NO2
8*12 + 9*1.00783 + 14.0031 + 2*15.9949 = 151.06337 g/mol
Step 4: Calculate molar mass of C10H17N
10*12 + 17*1.00783 + 14.0031 = 151.13621 g/mol
The molecular formula of X is C8H9NO2
