Answer:
(B.) and (C.)
b. So that clean NMR spectra can be obtained that do not contain solvent peaks.
c. So that the yield can be determined.
Explanation:
The solvent used in Nuclear Magnetic Resonance (NMR) spectrometer is Trimethyl silane (TMS), a neutral solvent which doesn't give off any signals. Other solvents could have interactions with the radiation, and disrupt the spectra.
Furthermore, for accurate determination of the actual yield and overall percentage yield, solid must be separated from the solvent, dried and weighed.
I hope this was explanatory enough.
Answer:
The empirical formula of a compound is Na2Cr2O7
Explanation:
Empirical formula is defined as the lowest ratio of elements present in any substance. In order to determine the empirical formula for a substance containing these elements we have to follow some steps.
1.In the first step, we have to divide the given mass of an element with its molecular mass to convert the mass to moles.

Similarly, the moles of Cr and O in that compound were calculated and found as 0.396 and 1.3875, respectively.
2. Then the next step is to determine the lowest moles and divide all the moles with that lowest mole. As here the lowest mole is 0.396. So on dividing the moles of Na, Cr and O with 0.396, we will obtain the ratio as 1:1:3.5.
3. As the ratio consists of a fractional number, we have to multiply it with the smallest possible integer to convert it to whole number. In this case, if we multiply it with 2 , we will get the ratio as 2:2:7.
Thus, the empirical formula for the compound can be written as Na2Cr2O7.