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snow_lady [41]
3 years ago
5

The following is a list of common errors encountered in research laboratories. Categorize each as a determinate or an indetermin

ate error, and further categorize determinate errors as instrumental, operative, or methodic:
(a) An unknown being weighed is hygroscopic.
(b) One component of a mixture being analyzed quantitatively by gas chromatography reacts with the column packing.
(c) The tip of the pipet used in the analysis is broken.
(d) In measuring the same peak heights of a chromatogram, two technicians each report different heights.
Chemistry
1 answer:
Kay [80]3 years ago
4 0

Answer:

An unknown being weighed is hygroscopic. - operative error

One component of a mixture being analyzed quantitatively by gas chromatography reacts with the column packing. - methodic error

The tip of the pipet used in the analysis is broken. - instrumental error

In measuring the same peak heights of a chromatogram, two technicians each report different heights - operative error

Explanation:

In chemical analysis, operative errors are that largely introduced into the measurement because of variation of personal judgements of analysts. It is also a personal error that emanates solely due to the analyst.

A methodic error arises as a result of adopting defective experimental methods. For example, a column packing that reacts with a component of the mixture is used in the gas chromatography.

Instrument error refers to the error of a measuring instrument, for instance, the use of a pipette with a broken tip.

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i. The given compound X is 2-methyl pent-2-ene. When it is reacted with ozone it forms an ozonide in the first step. In the second step the reduce to forms acetone and propanal.

ii. The structural formula of Y is CH_3-CO-CH_3 and Z is CH_3-CH_2-CHO.

iii. Alkenes, upon catalytic hydrogenation, form alkanes. This will occur in the presence of Nickel as the catalyst.

iv. The process of ozonolysis is useful in the field of pharmaceutics.

v. The test of unsaturation can be performed by passing a compound through Bromine water.

<h3>What is ozonolysis?</h3>

Ozonolysis is a reaction used in organic chemistry to determine the position of a carbon-carbon double bond in unsaturated compounds.

i. The given alkene X, that is subject to ozonolysis would be 2-methyl-2-pentene. Upon exposure to ozone, an ozonide is initially formed, after which it is broken down into 2 products - acetone and propanal, both with the molecular formula C₃H₆O.

The given compound X is 2-methyl pent-2-ene. When it is reacted with ozone it forms an ozonide in the first step. In the second step the reduce to forms acetone and propanal.

ii. The formulas of Y is CH_3-CO-CH_3 and Z is CH_3-CH_2-CHO. They are functional isomers as they have the same molecular formula but different functional groups - ketone and aldehyde.

iii. When alkenes undergo catalytic hydrogenation, they form alkanes, X will form 2 methyl petane on reaction with hydrogen gas in presence of Ni.

iv. The ozonolysis is used for the industrial-scale synthesis of pharmaceuticals.

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2 years ago
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2. 2

3. 3

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