Add 1 tsp. of vinegar to the canister at a time, filling it almost to the top. You need to add as much vinegar to the canister as possible without the vinegar and the baking soda coming into contact when you later snap the lid onto the canister. Depending on the exact canister, this may be around 5 tsp.
I believe distillation is used to separate solvents of different kind as long as it is heated to its boiling temp
₁₇Cl 1s²2s²2p⁶3s²3p⁵, 1 unpaired electron in 3pz orbital.