I think this is the solution:
1: U-1, F,-4
2: Na-6, Mo-1, O-4
3: Bi-1, O-1, C-1, I-1
4: In-9, N-1
5: N-2, H-4, S-1, C-1
6: Ge- 15, N-4
7: N-1, H-4, C-1, I-1, O-3
8: H-7, F-1
9: N-1, O-5, H-1, S-1
10: H-8
11: Nb-1, O-1, C-1, I-3
12: C-3, F-3, S-1, O-3, H-1
13: Ag-1, C-1, N-1, O-1
14: Pb-6, H-1, As-1, O-4
Choices 'C' and 'D' are both correct.
(Except in 'C', changing the temperature from 1°C to 3°C is not usually
described as 'cooling', and it's not the water's 'mass' that changes. But
water does contract in volume during that change.)