The sample must be sufficiently soluble (fig. 2) to yield an NMR spectrum. For 1H and 1H observed NMR, it is recommended to dissolve between 2 and 10 mg in between 0.6 and 1 mL of solvent so that the sample depth is at least 4.5 cm in the tube (fig. 3).
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The amount of precipitate produced will be proportional to the amount of NH₃ reacted with water to produce NH₄OH.
<h3>What is precipitate?</h3>
Precipitates are the crystal type formation, when the solute is no more dissolving in the solvent.
Imagine mixing 1 tablespoon of Epsom salt with 2 cups of ammonia, the reaction is
2NH₃ + MgSO₄ + 2H₂O → Mg(OH)₂ + (NH₄)₂SO₄
The amount of precipitate produced will be proportional to the amount of NH₃ reacted with water to produce NH₄OH.
Learn more about precipitate.
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