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o-na [289]
3 years ago
5

1. After clamping a buret to a ring stand, you notice that the set-up is tippy and unstable. What should you do to stabilize the

set-up?
A. Move the buret clamp to a ring stand with a larger base.
B. Hold the buret in place by hand during the titration.
C. Use a different size buret that is more stable in the set-up
D. Clamp another buret to the ring stand to balance out the set-up.
Chemistry
1 answer:
vampirchik [111]3 years ago
7 0

Answer:

A. Move the buret clamp to a ring stand with a larger base.

Explanation:

The ring stands are used to hold burettes, light in weight to avoid loss of stability, that is why it is necessary to change the size of the ring stand so that it can support the buret that we are going to use.  It is not recommended to balance it with the hand since it would give us an inaccurate result in the titration.

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8 0
3 years ago
Calculate the theoretical yield of aspirin obtained when 2.0 g of salicylic acid and 5.0 mL of acetic anhydride (density = 1.08
saw5 [17]

Answer:

The percent yield would be 73%

Explanation:

The balanced reaction for the obtention of acetylsalicylic acid (aspirin) is the following:

Salicylic acid + acetic anhydride → acetylsalicylic acid + acetic acid

C₇H₆O₃          +          C₄H₆O₃        →         C₉H₈O₄           +    C₂H₄O₂

According to the reaction, 1 mol of salicylic acid reacts with 1 mol of acetic anhydride to give 1 mol of acetylsalicylic acid (aspirin) and 1 mol of acetic acid.

1 mol aspirin (C₉H₈O₄) = (9 x 12 g/mol) + (8 x 1 g/mol) + (4 x 16 g/mol)

                                     = 180 g

1 mol salicylic acid (C₇H₆O₃) = (7 x 12 g/mol) + (6 x 1 g/mol) + (3 x 16 g/mol)

                                              = 138 g

1 mol acetic anhydride (C₄H₆O₃) = (4 x 12 g/mol) + (6 x 1 g/mol) + (3 x 16 g/mol)

                                                      = 102 g

The stoichiometric ratio is = 138 g salicylic acid/102 g acetic anhydride= 1.35

We have:

2.0 g salicylic acid

acetic anhydride = 5.0 mL x 1.08 g/mL = 5.4 g

The reactants ratio is = 2.0 g salicylic acid/5.4 g acetic anhydride = 0.37

0.37 < 1.35 , therefore <em>salicylic acid is the limiting reactant</em>.

Now, we use the amount of salicylic acid to calculate the theoretical amount of aspirin. For this, we know that 1 mol of aspirin (180 g) is obtained from 1 mol of salycilic acid (138 g):

theoretical yield= 180 g aspirin/138 g salycilic acid x 2.0 g salycilic acid = 2.61 g aspirin

actual yield = 1.9 g

Finally, we calculate the yield:

percent yield = actual yield/theoretical yield x 100

        = 1.9 g/2.6 g x 100 = 72.8% ≅ 73%

6 0
2 years ago
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